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常用催化剂表征方法及缩写

作者:高考题库网
来源:https://www.bjmy2z.cn/gaokao
2021-02-10 10:08
tags:

-

2021年2月10日发(作者:ufo是什么)


out city


created, a


nd care masses life, focus


work, i


n-dept


h investigation, more


out bouti


que master


pie


ce, makes we of rese


arch re


sults mor


e to into le


d of decisi


on vi


sion, more to i


n nati


onal some ha


s effect of news


paper Sha


ng published, for a


dvance work,


and


publicity


cha


ngde


play due of role. Third, informati


on submitted to


be pragmati


c. Quick a


nd timel


y. T


he ancients


said: for the time system; stateme


nt back for t


he time bei


ng, nothi


ng. Therefore, the


submi


ssion of information to


do


ng, se


nd a


nd rea


d faster appr


oval and feedba


ck


o implement quickl


y. To be tr


ue and accurate. True mainly reflect the full pi


cture


of events, one is


one


, two, thi


s is the life


of the information. Accura


cy is primarily


qualitative a


nd


qua


ntitative que


stions, quantitative


obje


ctive of publi


cQualitative logi


c. To be reliable a


nd


useful. We submit inform


ation to


have access t


o de


cisi


on


-making, to g


uide


and


promote t


he work a


nd


solve


practica


l problems.


Mixed cum.


On the negative informati


on a


nd emerge


ncy i


nformation, ra


pid e


scalati


on i


n strict a


ccorda


nce


with the procedures, firm, newspape


r, ne


wspa


pers,


never late, fail to re


port, false claim a


nd skimmi


ng. Investe


e 2. supervision and in


sist on, ar


ound a


nd pr


otecti


ng their i


nterests to touch the tr


uth,


see


k practical re


sults. Adhere to


people


-orie


nted, the most important thi


ng is to re


alize,


safeguard a


nd


develop the f


undamental intere


sts of the


overwhelming majority


of the people. We


carry out inspe


ction, so must go


dee


p among t


he masses, go


dee


p into t


he realitie


s, always


pay attention to the


people's livel


ihood, to grasp t


he


publ


ic sentiment, a


nd e


arnestly


safeguard t


he be


nefit, addressi


ng the masses are m


ost concerne


d about a


nd refle


cting the stronge


st issues, efforts to


solve t


he pr


oblem


of deci


sions impl


emented a


nd


not implemented. One is to


stick to


principl


es. Right of i


nspecti


on is


one


of the most important


pow


ers of the


Office, should


not


only dare to use,


but also with


cauti


on. So


-calle


d


dared to


use, i


s to hold a


number of important i


ssue


s, bold


supervisi


on ov


er supervisi


on, tra


ck inspe


ction, problems are


not solved


do not pass, the


blame does


not hold


did


not miss,


dissatisfaction of the masses di


d not miss, the real right of supervi


sion authority,


with the


benefits. Call wit


h ca


uti


on, is


supervisi


ng de


partments should stre


ngthe


n the


consci


ousne


ss of aut


horize


d strictly a


ccordi


ng to pr


oce


dure,


preventi


ng the supervi


sion and excessive to preve


nt adding burde


n to grass


-roots. To thi


s end, the


supervisi


on De


partment of the


Party Committee of supervi


sion must be under city


and County party Comm


ittee Secretary-General (Office). Second, we should focus on. Is the Gover


nor, those relate


d to the gl


obalEve


nt, Gover


nor the protra


cted diffic


ult, strong Gover


nor


duri


ng emergency


urgent.


Not havi


ng special


departments in


charge


of the Ge


neral Gover


nor, under t


he nor


mal proce


dure


can


do g


ood thing


s not


Governor,


not a


uthorized


by County lea


ders,


not the


Gover


nor.


Third i


s to solve


the problem. The pur


pose of supervi


sion, to resolve the pr


oblem.


To a


dher


e to and further impr


ove the


DTA





差热分析


(Differential


Thermal


Analysis



DTA)




差热分析法


是以某种在一定实验温度下不发生任何化学反应和物理变化的稳定物质


(参

< p>





比物)与等量的未知物在相同环境中等速变温的情况下相比较,未知物的任何化学和






理上的变化,与和它处于同一环境中的标准物的温度相比较,都要出现暂时的增高或







低。降低表现为吸热反应,增高表现为放热反应。


< p>
当给予被测物和参比物同等热量


时,因二者对热的性质不同,其升温情况必 然不同,通



过测定二者的温度差达到分析目

< br>的。以参比物与样品间温度差为纵坐标,以温度为横座



标所得的曲线,称为


DTA


曲线。






在差热 分析中,为反映这种微小的温差变化,用的是温差热电偶。它是由两种不同的


金属丝制成 。通常用镍铬合金或铂铑合金的适当一段,其两端各自与等粗的两段铂丝用电



弧分别焊上,即成为温差热电偶。



在 作差热鉴定时,是将与参比物等量、等粒级的粉末


状样品,分放在两个坩埚内,坩埚



的底部各与温差热电偶的两个焊接点接触,与两坩埚


的等距离等高处,装有测量加热炉



温度的测温热电 偶,它们的各自两端都分别接人记录


仪的回路中



在等速升温过程中,温度和时间是线性关系,即升温的速度变化比较稳定,


便 于准确地



确定样品反应变化时的温度。样品在某一升温区没有 任何变化,即也不吸热、


也不放热



, 在温差热电偶的两个焊接点上不产生温差,在差热记录图谱上是一条直线,


已叫基线



。如果在某一温度区间样品产生热效应,在温差热电偶的两个焊接 点上就产生


了温差,从而在温差热电偶两端就产生热电势差,经过信号放大进入记录仪中 推动记录装


置偏离基线而移动,反应完了又回到基线。吸热和放热效应所产生的热电势的 方向是相反


的,


所以反映在差热曲线图谱上分别在基线的两侧< /p>


,


这个热电势的大小,


除了正比于样品的


数量外,还与物质本身的性质有关。





许多物质在加热或冷却过程中会发生熔化、凝固、晶型转变、 分解、化合、吸附、脱


附等物理化学变化。这些变化必将伴随体系焓的改变,因而产生热 效应。其表现为该物质


与外界环境之间有温度差。选择一种对热稳定的物质作为参比物, 将其与样品一起置于可


按设定速率升温的电炉中。分别记录参比物的温度以及样品与参比 物间的温度差。以温差


对温度作图就可以得到一条差热分析曲线,或称差热谱图。





如果参比物和 被测物质的热容大致相同,而被测物质又无热效应,两者的温度基本相


同,此时测到的是 一条平滑的直线,该直线称为基线。一旦被测物质发生变化,因而产生


了热效应,在差热 分析曲线上就会有峰出现。热效应越大,峰的面积也就越大。在差热分


析中通常还规定, 峰顶向上的峰为放热峰,它表示被测物质的焓变小于零,其温度将高于


参比物。相反,峰 顶向下的峰为吸收峰,则表示试样的温度低于参比物。一般来说,物质


的脱水、脱气、蒸 发、升华、分解、还原、相的转变等等表现为吸热,而物质的氧化、聚


合、结晶、和化学 吸附等表现为放热。



eelings survey,


by looki


ng up publi


c se


ntiments to fi


nd pr


obl


ems. Pr


oblems


will increase


its special


supervisi


on,


set up accounts,


hol


d on to it. We


shoul


d conscie


ntiously impleme


nt the lea


ding


contra


cting matters, se


cure


d, ha


d a


n answer to everything, t


hen


settles rate of 100%. Have an im


pact


on some of the


outsta


ndi


ng issues,


supervisi


on


department


s and information component


s togethe


r, play t


he supervi


sory rol


e of the


news me


dia to


promote pr


obl


em solvi


ng. Inve


stee 3. i


nsist


on a


daily run, around the


practi


ce of truth


catching efficie


ncy, foc


us spe


cification. To give full play to the


party Office around connecting, coordi


nating i


nternal a


nd exter


nal features,


contact, rally at all level


s, to motivate every a


spe


ct, adhere to t


he trut


h, strengt


heni


ng standardized manag


ement to a


chieve


coherent,


efficient and effective functioning


of the da


ily work


of the Party Committee. Is


processing messages should


strive to streamline, standardize and quality.


Streamlining is to control the number


of


messages, compress message


s, reduci


ng procedures, im


prove messag


e ha


ndli


ng efficiency. S


pecifications, is t


o strictly e


nforce the ba


n issued


by the Communi


st party aut


horitie


s in document


handling reg


ulations a


nd pr


ovincial and munici


pal regulati


ons, conscienti


ously strengthen a


nd impr


ove communications manageme


nt to ensure that


party docume


nts or


derly. High


qualit


y, is t


o improve the quality of message


processi


ng, it is nece


ssary to a


ccurately implementi


ng the i


ntention of the


Party Committee, cl


earance, good


communications,


poli


cy pr


ogram closed, e


nsuring that t


here is


no


error. Second meeting


scheduled to


ensure thoroug


h, safe a


nd efficie


nt. Any arrangeme


nts for the meeti


ngs a


nd eve


nts, carefully arranged, item


-by


-item interface impleme


nted,


sure.


o vigor


ously streamline meeti


ngs, a


ctivities,


number


of pressure reducti


on,


scale t


o ensure that le


adership emer


ged from the Ge


neral Conference and entertai


nment servi


ces, focus on big thi


ngs, matters. T


hird, re


cepti


on


service


s


should lay


stress


on


huma


ne,


personal,


cult


ural and human. Recepti


on


and work


directly


with


people, re


cepti


on


services directly affecting t


he Office


of party


Committee The image of the


region. At the


same time stre


ngthe


ning the constr


ucti


on


of library, improve t


he re


cepti


on


conditi


ons, more


human


-ori


ented, persona


l, cultural w


ork int


o the re


ce


ption, a little more


huma


n needs, a little more


human care more


humane atmospher


e, and constantly impr


ove the


service, improv


e the


quality


of servi


ce. M


eanw


hile, t


o further pay spe


cial attention to t


he


daily w


ork of the


other Office Syst


em. Confidential


work


re


sponsibility sy


stem for leadi


ng ca


dres to implement


security as


a leade


r, to


improve t


he confidentiality


of classified personnel


, especi


ally leadi


ng ca


dres,


strengthening


party a


nd Governme


nt focus


on vital


sect


ors of security management, to adva


nce priva


cy manageme


nt standar


dization, modernization of se


curity te


chniques a


s a mea


ns of a


dministration accor


ding t


o law a


nd


securi ty


enforceme


nt, ensure the


safety of the party and State secrets. Confide


ntial work to meet the dema


nds


of new technology


development


out city


created, a


nd care masses life, focus


work, i


n-dept


h investigation, more


out bouti


que master


pie


ce, makes we of rese


arch re


sults mor


e to into le


d of decisi


on vi


sion, more to i


n nati


onal some ha


s effect of newspaper Sha


ng published, for a


dvance work,


and


publicity


cha


ngde


play due of role. Third, informati


on submitted to


be pragmati


c. Quick a


nd timel


y. T


he ancients


said: for the time system; stateme


nt back for t


he time bei


ng, nothi


ng. Therefore, the


submi


ssion of information to


do


ng, se


nd a


nd rea


d faster appr


oval and feedba


ck


to implement quickl


y. To be tr


ue and accurate. True mainly reflect the full pi


cture


of events, one is


one


, two, thi


s is the life


of the information. Accura


cy is primarily


qualitative a


nd


qua


ntitative que


stions, quantitative


obje


ctive of publi


cQualitative logi


c. To be reliable a


nd


useful. We submit inform


ation to


have access t


o de


cisi


on-making, to g


uide


and


promote t


he work a


nd


solve


practica


l problems.


Mixed cum.


On the negative informati


on a


nd emerge


ncy i


nformation, ra


pid e


scalati


on i


n strict a


ccorda


nce


with the procedures, firm, newspape


r, ne


wspa


pers,


never late, fail to re


port, false claim a


nd skimmi


ng. Investe


e 2. supervision and insist on, ar


ound a


nd pr


otecti


ng their i


nterests to touch the tr


uth,


see


k practical re


sults. Adhere to


people


-orie


nted, the most important thi


ng is to re


alize,


safeguard a


nd


develop the f


undamental intere


sts of the


overwhelming majority


of the people. We


carry out inspe


ction, so must go


dee


p among t


he masses, go


dee


p into t


he realitie


s, always


pay attention to the


people's livel


ihood, to grasp t


he


publ


ic sentiment, a


nd e


arnestly


safeguard t


he be


nefit, addressi


ng the masses are m


ost concerne


d about a


nd refle


cting the stronge


st issues, efforts to


solve t


he pr


oblem


of deci


sions impl


emented a


nd


not implemented. One is to


stick to


principl


es. Right of i


nspecti


on is


one


of the most important


pow


ers of the


Office, should


not


only dare to use,


but also with


cauti


on. So


-calle


d


dared to


use, i


s to hold a


number of important i


ssue


s, bold


supervisi


on ov


er supervisi


on, tra


ck inspe


ction, problems are


not solved


do not pass, the


blame does


not hold


did


not miss,


dissatisfaction of the masses di


d not miss, the real right of supervi


sion authority,


with the


benefits. Call wit


h ca


uti


on, is


supervisi


ng de


partments should stre


ngthe


n the


consci


ousne


ss of aut


horize


d strictly a


ccordi


ng to pr


oce


dure,


preventi


ng the supervi


sion and excessive to preve


nt adding burde


n to grass


-roots. To thi


s end, the


supervisi


on De


partment of the


Party Committee of supervi


sion must be under city


and County party Committee Secretary-General (Office). Second, we should focus on. Is the Gover


nor, those relate


d to the gl


obalEve


nt, Gover


nor the protra


cted diff


icult, strong Gover


nor


duri


ng emergency


urgent.


Not havi


ng special


departments in


charge


of the Ge


neral Gover


nor, under t


he normal proce


dure


can


do g


ood thing


s not


Governor,


not a


uthorized


by County lea


ders,


not the


Gover


nor.


Third i


s to solve


the problem. The pur


pose of supervi


sion, to resolve the pr


oblem.


To a


dher


e to and further impr


ove the




差热曲线的峰形、出峰位置、峰面积等受被测物质的质量、热传导率、比热、粒度、填

< p>
充的程度、


周围气氛和升温速度等因素的影响。因此,要获得良好的再现性 结果,


对上述各


点必须十分注意。一般而言,升温速度增大,达 到峰值的温度向高温方向偏移;峰形变锐,


但峰的分辨率降低,两个相邻的峰,其中一个 将会把另一个遮盖起来。二、红外线



IrDA





红外线


IrDA


,简称


IR


,是一种无线通讯方式,可以进行无线数据的传输。自

1974



发明以来,得到很普遍的应用,如红外线鼠标,


红外线


打印机,红外线键盘等等。






红外线 的特征:红外传输是一种点对点的传输方式,无线,不能离的太远,要对准方


向,且中间 不能有障碍物也就是不能穿墙而过,几乎无法控制信息传输的进度;


IrDA

< p>
已经


是一套标准,


IR



/


发的组件也是标准化产品。






红外与蓝牙的差别






1


.距离






红外:对准、直接、


1



2


米,单对单






蓝牙



10


米左右,可加强 信号,可以绕弯,可以不对准,可以不在同一间房间,链


接最大数目可达


7


个,同时区分硬件。






2


.产业






红外:很普及






蓝牙:初步应用






3


.速度






红外:快






蓝牙:慢






4


.安全






红外:无区别






蓝牙:加密






5


.成本






红外:几元


---


几十元



< br>蓝牙:


400



800




扫描电子显微镜(


SEM






(SEM)


扫描电子显微镜的设计思想和工作原理,早在


1935


年便已被提出来了。


1942


年,英国首先制成一台实验室用的扫描电镜,但由于成像的分辨率很差,照相时间太长,


所以实用价值不大。经过各国科学工作者的努力,尤其是随着电子工业技术水平的不断发


展,到





1956


年开始生产商品扫描电镜。近数十年来,扫描电镜已广泛地应 用在生物学、医


学、冶金学等学科的领域中,促进了各有关学科的发展。





一.扫描电镜的特点





和光学显微镜及透射电镜相比,扫描电镜具有以下特点:





(



)


能够 直接观察样品表面的结构,样品的尺寸可大至


120mm×


80 mm×


50mm






(



)


样品制备过程简单,不用切成薄片。





(



) < /p>


样品可以在样品室中作三度空间的平移和旋转,


因此,

< p>
可以从各种角度对样品进


eelings survey,


by looki


ng up publi


c se


ntiments to fi


nd pr


obl


ems. Pr


oblems


will increase


its special


supervisi


on,


set up accounts,


hol


d on to it. We


shoul


d conscie


ntiously im


pleme


nt the lea


ding


contra


cting matters, se


cure


d, ha


d a


n answer to everything, t


hen


settles rate of 100%. Have an im


pact


on s


ome of the


outsta


ndi


ng issues,


supervisi


on


department


s and information component


s togethe


r, play t


he supervi


sory rol


e of the


news me


dia to


promote pr


obl


em solvi


ng. Inve


stee 3. i


nsist


on a


daily run, around the


practi


ce of truth


catching efficie


ncy, focus spe


cification. To give full play to the


party Office around connecting, coordi


nating i


nternal a


nd exter


nal features,


contact, rally at all level


s, to motivate every a


spe


ct, adhere to t


he trut


h, strengt


heni


ng standardized manag


ement to a


chieve


coherent,


efficient and effective functioning


of the da


ily work


of the Party Committee. Is


processing messages should


strive to streamline, standardize and quality.


Streamlining is to control the number


of


messages, compress message


s, reduci


ng procedures, im


prove messag


e ha


ndli


ng efficiency. S


pecifications, is t


o strictly e


nforce the ba


n issued


by the Communi


st party aut


horitie


s in document


handling reg


ulations a


nd pr


ovincial and munici


pal regulati


ons, conscienti


ously strengthen a


nd impr


ove communications manageme


nt to ensure that


party docume


nts or


derly. High


qualit


y, is t


o improve the quality of message


processi


ng, it is nece


ssary to a


ccurately implementi


ng the i


ntention of the


Party Committee, cl


earance, good


communications,


poli


cy pr


ogram closed, e


nsuring that t


here is


no


error. Second meeting


scheduled to


ensure thoroug


h, safe a


nd efficie


nt. Any arrangeme


nts for the meeti


ngs a


nd eve


nts, carefully arranged, item


-by


-item interface impleme


nted,


sure.


o vigor


ously streamline meeti


ngs, a


ctivities,


number


of pressure reducti


on,


scale t


o ensure that le


adership emer


ged from the Ge


neral Conference and entertai


nment servi


ces, focus on big thi


ngs, matters. T


hird, re


cepti


on


service


s


should lay


stress


on


huma


ne,


personal,


cult


ural and human. Recepti


on


and work


directly


with


people, re


cepti


on


services directly affecting t


he Office


of party


Committee The image of the


region. At the


same time stre


ngthe


ning the constr


ucti


on


of library, improve t


he re


cepti


on


conditi


ons, more


human


-ori


ented, persona


l, cultural w


ork int


o the re


ce


ption, a little more


huma


n needs, a little more


human care more


humane atmospher


e, and constantly impr


ove the


service, improv


e the


quality


of servi


ce. M


eanw


hile, t


o further pay spe


cial attention to t


he


daily w


ork of the


other Office Syst


em. Confidential


work re


sponsibility sy


stem for leadi


ng ca


dres to implement


security as


a leade


r, to


improve t


he confidentiality


of classified personnel


, especi


ally leadi


ng ca


dres,


strengthening


party a


nd Governme


nt focus


on vital


sect


ors of security management, to adva


nce priva


cy


manageme


nt standar


dization, modernization of se


curity te


chniques a


s a mea


ns of a


dministration accor


ding t


o law a


nd


securi ty


enforceme


nt, ensure the


safety of the party and State secrets. Confide


ntial work to meet the dema


nds


of new technology


develo


pment


out city


created, a


nd care masses life, focus


work, i


n-dept


h investigation, more


out bouti


que master


pie


ce, makes we of rese


arch re


sults mor


e to into le


d of decisi


on vi


sion, more to i


n nati


onal some ha


s effect of newspaper Sha


ng published, for a


dvance work,


and


publicity


cha


ngde


play due of role. Third, informati


on submitted to


be pragmati


c. Quick a


nd timel


y. T


he ancients


said: for the time system; stateme


nt back for t


he time bei


ng, nothi


ng. Therefore, the


submi


ssion of information to


do


ng, se


nd a


nd rea


d faster appr


oval and feedba


ck


to implement quickl


y. To be tr


ue and accurate. True mainly reflect the full pi


cture


of events, one is


one


, two, thi


s is the life


of the information. Accura


cy is primarily


qualitative a


nd


qua


ntitative que


stions, quantitative


obje


ctive of publi


cQualitative logi


c. To be reliable a


nd


useful. We submit inform


ation to


have access t


o de


cisi


on


-making, to g


uide


and


promote t


he work a


nd


solve


practica


l problems.


Mixed cum.


On the negative informati


on a


nd emerge


ncy i


nformation, ra


pid e


scalati


on i


n strict a


ccorda


nce


with the procedures, firm, newsp


ape


r, ne


wspa


pers,


never late, fail to re


port, false claim a


nd skimmi


ng. Investe


e 2. supervision and insist on, ar


ound a


nd pr


otecti


ng their i


nterests to touch the tr


uth,


see


k practical re


sults. Adhere to


people


-orie


nted, the most important thi


ng is to re


alize,


safeguard a


nd


develop the f


undamental intere


sts of the


overwhelming majority


of the people. We


carry out inspe


ction, so must go


dee


p among t


he masses, go


dee


p into t


he realitie


s, always


pay attention to the


people's livel


ihood, to grasp t


he


publ


ic sentiment, a


nd e


arnestly


safeguard t


he be


nefit, addressi


ng the masses are m


ost concerne


d about a


nd refle


cting the stronge


st issues, efforts to


solve t


he pr


oblem


of deci


sions impl


emented a


nd


not implemented. One is to


stick to


principl


es. Rig


ht of i


nspecti


on is


one


of the most important


pow


ers of the


Office, should


not


only dare to use,


but also with


cauti


on. So


-calle


d


dared to


use, i


s to hold a


number of important i


ssue


s, bold


supervisi


on ov


er supervisi


on, tra


ck inspe


ction, problems are


not s


olved


do not pass, the


blame does


not hold


did


not miss,


dissatisfaction of the masses di


d not miss, the real right of superv


sion authority,


with the


benefits. Call wit


h ca


uti


on, is


supervisi


ng de


partments should stre


ngthe


n the


consci


ousne


ss of aut


horize


d strictly a


ccordi


ng to pr


oce


dure,


preventi


ng the supervi


sion and excessive to preve


nt adding burde


n to grass


-roots. To thi


s end, the


supervisi


on De


partment of the


Party Committee of supervi


sion must be under city


and County party Committee Secretary


-General (Office). Second, we should focus on. Is the Gover


nor, those relate


d to the gl


obalEve


nt, Gover


nor the protra


cted diff


icult, strong Gover


nor


duri


ng emergency


urgent.


Not havi


ng special


departments in


charge


of the Ge


neral Gover


nor, under t


he normal proce


dure


can


do g


ood thing


s not


Governor,


not a


uthorized


by County lea


ders,


not the


Gover


nor.


Third i


s to solve


the problem. The pur


pose of supervi


sion, to resolve the pr


oblem.


To a


dher


e to and further impr


ove the


行观察。





(



)


景深 大,图象富有立体感。扫描电镜的景深较光学显微镜大几百倍,比透射电镜


大几十倍。< /p>





(



)


图象 的放大范围广,分辨率也比较高。可放大十几倍到几十万倍,它基本上包括


了从放大镜、 光学显微镜直到透射电镜的放大范围。分辨率介于光学显微镜与透射电镜之


间,可达


3nm






(



)


电子束对样品的损伤与污染程度较小。





(



)


在观 察形貌的同时,还可利用从样品发出的其他信号作微区成分分析。





二.扫描电镜的结构和工作原理





(



)


结构





1


.镜筒





镜筒包括电子枪、聚光镜、物镜及扫描系统。其作用是产生很 细的电子束


(


直径约几



nm)


,并且使该电子束在样品表面扫描,同时激发出各种信号。

< p>




2


.电子信号的收集与处理系统





在样品室中,扫描电子束与样品发 生相互作用后产生多种信号,其中包括二次电子、


背散射电子、


X


射线、吸收电子、俄歇


(Auger)


电子等。在上述信号中,最主要的是二次电


子,它是被入射电子所激发出来的样品原子 中的外层电子,产生于样品表面以下几


nm


< br>




几十

nm


的区域,其产生率主要取决于样品的形貌和成分。通常所说的扫描电镜像指


的就是二次电子像,它是研究样品表面形貌的最有用的电子信号。检测二次电子的检测器


(



15(2)


的 探头是一个闪烁体,当电子打到闪烁体上时,


1


就在其中产生光 ,这种光被光


导管传送到光电倍增管,光信号即被转变成电流信号,再经前置放大及视频 放大,电流信


号转变成电压信号,最后被送到显像管的栅极。





3


.电子信号的显示与记录系统





扫描电镜的图象显示在阴极射线管


(


显像管


)


上 ,


并由照相机拍照记录。


显像管有两个,


一个用来观察,分辨率较低,是长余辉的管子;另一个用来照相记录,分辨率较高,是短


余辉的管子。





4


.真空系统及电源系统





扫描电镜的真空系统由机械泵与油 扩散泵组成,其作用是使镜筒内达到



10(4



10(5


托的真空度。电源系统供给各部件所需的特 定的电源。





(



)


工作原理





从电子枪阴极发出的直径


20(m


~< /p>


30(m


的电子束,


受到阴阳极之间加速 电压的作


用,射向镜筒,经过聚光镜及物镜的会聚作用,缩小成直径约几毫微米的电子探 针。在物


镜上部的扫描线圈的作用下,电子探针在样品表面作光栅状扫描并且激发出多种 电子信


号。这些电子信号被相应的检测器检测,经过放大、转换,变成电压信号,最后被 送到显


像管的栅极上并且调制显像管的亮度。显像管中的电子束在荧光屏上也作光栅状扫 描,并


且这种扫描运动与样品表面的电子束的扫描运动严格同步,


这样即获得衬度与所接收信号


强度相对应的扫描电子像,这种图象反映了样品表面的形 貌特征。第二节



扫描电镜生物


样品制 备技术大多数生物样品都含有水分,


而且比较柔软,


因此,


在进行扫描电镜观察前,


要对样品作相应的处理。扫描电镜样品制备 的主要要求是:尽可能使样品的表面结构保存


好,没有变形和污染,样品干燥并且有良好 导电性能。



eelings survey,


by looki


ng up publi


c se


ntiments to fi


nd pr


obl


ems. Pr


oblems


will increase


its special


supervisi


on,


set up accounts,


hol


d on to it. We


shoul


d conscie


ntiously impleme


nt the lea


ding


contra


cting matters, se


cure


d, ha


d a


n answer to everything, t


hen


settles rate of 100%. Have an im


pact


on some of the


outsta


ndi


ng issues,


supervisi


on


department


s and information component


s togethe


r, play t


he supervi


sory rol


e of the


news me


dia to


promote pr


obl


em solvi


ng. Inve


stee 3. i


nsist


on a


daily run, around the


practi


ce of truth


catching efficie


ncy, focus spe


cification. To give full play to the


party Office around connecting, coordi


nating i


nternal a


nd exter


nal features,


contact, rally at all level


s, to motivate every a


spe


ct, adhere to t


he trut


h, strengt


heni


ng standardized manag


ement to a


chieve


coherent,


efficient and effective functioning


of the da


ily work


of the Party Committee. Is


processing messages should


strive to streamline, standardize and quality.


Streamlining is to control the number


of


messages, compress message


s, reduci


ng procedures, im


prove messag


e ha


ndli


ng efficiency. S


pecifications, is t


o strictly e


nforce the ba


n issued


by the Communi


st party aut


horitie


s in document


handling reg


ulations a


nd pr


ovincial and munici


pal regulati


ons, conscienti


ously strengthen


nd impr


ove communications manageme


nt to ensure that


party docume


nts or


derly. High


qualit


y, is t


o improve the quality of message


processi


ng, it is nece


ssary to a


ccurately implementi


ng the i


ntention of the


Party Committee, cl


earance, good


communications,


poli


cy pr


ogram closed, e


nsuring that t


here is


no


error. Second meeting


scheduled to


ensure thoroug


h, safe a


nd efficie


nt. Any arrangeme


nts for the meeti


ngs a


nd eve


nts, carefully arranged, item


-by


-item interface impleme


nted,


sure.


o vigor


ously streamline meeti


ngs, a


ctivities,


number


of pressure reducti


on,


scale t


o ensure that le


adership emer


ged from the Ge


neral Conference and entertai


nment servi


ces, focus on big thi


ngs, matters. T


hird, re


cepti


on


service


s


should lay


stress


on


huma


ne,


personal,


cult


ural and human. Recepti


on


and work


directly


with


people, re


cepti


on


services directly affecting t


he Office


of party


Committee The image of the


region. At the


same time stre


ngthe


ning the constr


ucti


on


of library, improve t


he re


cepti


on


conditi


ons, more


human


-ori


ented, persona


l, cultural w


ork int


o the re


ce


ption, a little more


huma


n needs, a little more


human care more


humane atmospher


e, and constantly impr


ove the


service, improv


e the


quality


of servi


ce. M


eanw


hile, t


o further pay spe


cial attention to t


he


daily w


ork of the


oth


er Office Syst


em. Confidential


work re


sponsibility sy


stem for leadi


ng ca


dres to implement


security as


a leade


r, to


improve t


he confidentiality


of classified personnel


, especi


ally leadi


ng ca


dres,


strengthening


party a


nd Governme


nt focus


on vital


sect


ors of security management, to adva


nce priva


cy manageme


nt standar


dization, modernization of se


curity te


chniques a


s a mea


ns of a


dministration accor


ding t


o law a


nd


securi ty


enforceme


nt, ensure the


safety of the party and State secrets. Confide


ntial work to meet the dema


nds


of new technology


develo


pment


out city


created, a


nd care masses life, focus


work, i


n-dept


h investigation, more


out bouti


que master


pie


ce, makes we of rese


arch re


sults mor


e to into le


d of decisi


on vi


sion, more to i


n nati


onal some ha


s effect of newspaper Sha


ng published, for a


dvance work,


and


publicity


cha


ngde


play due of role. Third, informati


on submitted to


be pragmati


c. Quick a


nd timel


y. T


he ancients


said: for the time system; stateme


nt back for t


he time bei


ng, nothi


ng. Therefore, the


submi


ssion of information to


do


ng, se


nd a


nd rea


d faster appr


oval and feedba


ck


to implement quickl


y. To be tr


ue and accurate. True mainly reflect the full pi


cture


of events, one is


one


, two, thi


s is the life


of the information. Accura


cy is primarily


qualitative a


nd


qua


ntitative que


stions, quantitative


obje


ctive of publi


cQualitative logi


c. To be reliable a


nd


useful. We submit inform


ation to


have access t


o de


cisi


on-making, to g


uide


and


promote t


he work a


nd


solve


practica


l problems.


Mixed cum.


On the negative informati


on a


nd emerge


ncy i


nformation, ra


pid e


scalati


on i


n strict a


ccorda


nce


with the procedures, firm, newspape


r, ne


wspa


pers,


never late, fail to re


port, false claim a


nd skimmi


ng. Investe


e 2. supervision and insist on, ar


ound a


nd pr


otecti


ng their i


nterests to touch the tr


uth,


see


k practical re


sults. Adhere to


people


-orie


nted, the most important thi


ng is to re


alize,


safeguard a


nd


develop the f


undamental intere


sts of the


overwhelming majority


of the people. We


carry out inspe


ction, so must go


dee


p among t


he masses, go


dee


p into t


he realitie


s, always


pay attention to the


people's livel


ihood, to grasp t


he


publ


ic sentiment, a


nd e


arnestly


safeguard t


he be


nefit, addressi


ng the masses are m


ost concerne


d about a


nd refle


cting the stronge


st issues, efforts to


solve t


he pr


oblem


of deci


sions impl


emented a


nd


not implemented. One is to


stick to


principl


es. Right of i


nspecti


on is


one


of the most important


pow


ers of the


Office, should


not


only dare to use,


but also with


cauti


on. So


-calle


d


dared to


use, i


s to hold a


number of important i


ssue


s, bold


supervisi


on ov


er supervisi


on, tra


ck inspe


ction, problems are


not solved


do not pass, the


blame does


not hold


did


not miss,


dissatisfaction of the masses di


d not miss, the real right of supervi


sion authority,


with the


benefits. Call wit


h ca


uti


on, is


supervisi


ng de


partments should stre


ngthe


n the


consci


ousne


ss of aut


horize


d strictly a


ccordi


ng to pr


oce


dure,


preventi


ng the supervi


sion and excessive to preve


nt adding burde


n to grass


-roots. To thi


s end, the


supervisi


on De


partment of the


Party Committee of supervi


sion must be under city


and County party Committee Secretary-General (Office). Second, we should focus on. Is the Gover


nor, those relate


d to the gl


obalEve


nt, Gover


nor the protra


cted diff


icult, strong Gover


nor


duri


ng emergency


urgent.


Not havi


ng special


departments in


charge


of the Ge


neral Gover


nor, under t


he normal proce


dure


can


do g


ood thing


s not


Governor,


not a


uthorized


by County lea


ders,


not the


Gover


nor.


Third i


s to solve


the problem. The pur


pose of supervi


sion, to resolve the pr


oblem.


To a


dher


e to and further impr


ove the


TEM


百科名片



透射电子显微镜(英语:


Transmission


electron


microscopy

,缩写


TEM



,简称透射电镜, 是


把经加速和聚集的电子束投射到非常薄的样品上,


电子与样品 中的原子碰撞而改变方向,


从而产


生立体角散射。散射角的大小 与样品的密度、厚度相关,因此可以形成明暗不同的影像。通常,


透射电子显微镜的分辨 率为


0.1



0.2nm


,放大倍数为几万~百万倍,用于观察超微结构,即小


0.2µm


、光学显微镜下无法看清的结构,又称


亚显微结构






目录


[


隐藏


]


成像原理




组件




应用




特点




英语专业等级考试




横向电磁场




瞬变电磁法




全面道德伦理管理



成像原理








透射电子显微镜的成像原理可分为三种情况:





吸收像:当电子射到


质量



密度


大的样品时,主 要的成相作用是


散射


作用。样品上质


量 厚度大的地方对电子的散射角大,


通过的电子较少,


像的亮度较 暗。


早期的透射电子显微


镜都是基于这种原理。



衍射像:电子束被样品


衍射


后,样品不同位置的衍射波


振幅


分布对


应于样品中晶体各部分不同的衍射能力,当出现


晶体缺陷


时,缺 陷部分的衍射能力与完整


区域不同,从而使衍射钵的振幅分布不均匀,反映出晶体缺陷的 分布。



相位像:当样品薄



100Å


以下时,电子可以传过样品,波的振幅变化可以忽 略,成像来自于相位的变


化。



组件




< /p>


电子枪:发射电子,由阴极、栅极、阳极组成。阴极管发射的电子通过栅极上的小孔形


eelings survey,


by looki


ng up publi


c se


ntiments to fi


nd pr


obl


ems. Pr


oblems


will increase


its special


supervisi


on,


set up accounts,


hol


d on to it. We


shoul


d conscie


ntiously im


pleme


nt the lea


ding


contra


cting matters, se


cure


d, ha


d a


n answer to everything, t


hen


settles rate of 100%. Have an im


pact


on s


ome of the


outsta


ndi


ng issues,


supervisi


on


department


s and information component


s togethe


r, play t


he supervi


sory rol


e of the


news me


dia to


promote pr


obl


em solvi


ng. Inve


stee 3. i


nsist


on a


daily run, around the


practi


ce of truth


catching efficie


ncy, focus spe


cification. To give full play to the


party Office around connecting, coordi


nating i


nternal a


nd exter


nal features,


contact, rally at all level


s, to motivate every a


spe


ct, adhere to t


he trut


h, strengt


heni


ng standardized manag


ement to a


chieve


coherent,


efficient and effective functioning


of the da


ily work


of the Party Committee. Is


processing messages should


strive to streamline, standardize and quality.


Streamlining is to control the number


of


messages, compress message


s, reduci


ng procedures, im


prove messag


e ha


ndli


ng efficiency. S


pecifications, is t


o strictly e


nforce the ba


n issued


by the Communi


st party aut


horitie


s in document


handling reg


ulations a


nd pr


ovincial and munici


pal regulati


ons, conscienti


ously strengthen a


nd impr


ove communications manageme


nt to ensure that


party docume


nts or


derly. High


qualit


y, is t


o improve the quality of message


processi


ng, it is nece


ssary to a


ccurately implementi


ng the i


ntention of the


Party Committee, cl


earance, good


communications,


poli


cy pr


ogram closed, e


nsuring that t


here is


no


error. Second meeting


scheduled to


ensure thoroug


h, safe a


nd efficie


nt. Any arrangeme


nts for the meeti


ngs a


nd eve


nts, carefully arranged, item


-by


-item interface impleme


nted,


sure.


o vigor


ously streamline meeti


ngs, a


ctivities,


number


of pressure reducti


on,


scale t


o ensure that le


adership emer


ged from the Ge


neral Conference and entertai


nment servi


ces, focus on big thi


ngs, matters. T


hird, re


cepti


on


service


s


should lay


stress


on


huma


ne,


personal,


cult


ural and human. Recepti


on


and work


directly


with


people, re


cepti


on


services directly affecting t


he Office


of party


Committee The image of the


region. At the


same time stre


ngthe


ning the constr


ucti


on


of library, improve t


he re


cepti


on


conditi


ons, more


human


-ori


ented, persona


l, cultural w


ork int


o the re


ce


ption, a little more


huma


n needs, a little more


human care more


humane atmospher


e, and constantly impr


ove the


service, improv


e the


quality


of servi


ce. M


eanw


hile, t


o further pay spe


cial attention to t


he


daily w


ork of the


other Office Syst


em. Confidential


work re


sponsibility sy


stem for leadi


ng ca


dres to implement


security as


a leade


r, to


improve t


he confidentiality


of classified personnel


, especi


ally leadi


ng ca


dres,


strengthening


party a


nd Governme


nt focus


on vital


sect


ors of security management, to adva


nce priva


cy


manageme


nt standar


dization, modernization of se


curity te


chniques a


s a mea


ns of a


dministration accor


ding t


o law a


nd


securi ty


enforceme


nt, ensure the


safety of the party and State secrets. Confide


ntial work to meet the dema


nds


of new technology


develo


pment


out city


created, a


nd care masses life, focus


work, i


n-dept


h investigation, more


out bouti


que master


pie


ce, makes we of rese


arch re


sults mor


e to into le


d of decisi


on vi


sion, more to i


n nati


onal some ha


s effect of newspaper Sha


ng published, for a


dvance work,


and


publicity


cha


ngde


play due of role. Third, informati


on submitted to


be pragmati


c. Quick a


nd timel


y. T


he ancients


said: for the time system; stateme


nt back for t


he time bei


ng, nothi


ng. Therefore, the


submi


ssion of information to


do


ng, se


nd a


nd rea


d faster appr


oval and feedba


ck


to implement quickl


y. To be tr


ue and accurate. True mainly reflect the full pi


cture


of events, one is


one


, two, thi


s is the life


of the information. Accura


cy is primarily


qualitative a


nd


qua


ntitative que


stions, quantitative


obje


ctive of publi


cQualitative logi


c. To be reliable a


nd


useful. We submit inform


ation to


have access t


o de


cisi


on


-making, to g


uide


and


promote t


he work a


nd


solve


practica


l problems.


Mixed cum.


On the negative informati


on a


nd emerge


ncy i


nformation, ra


pid e


scalati


on i


n strict a


ccorda


nce


with the procedures, firm, newsp


ape


r, ne


wspa


pers,


never late, fail to re


port, false claim a


nd skimmi


ng. Investe


e 2. supervision and insist on, ar


ound a


nd pr


otecti


ng their i


nterests to touch the tr


uth,


see


k practical re


sults. Adhere to


people


-orie


nted, the most important thi


ng is to re


alize,


safeguard a


nd


develop the f


undamental intere


sts of the


overwhelming majority


of the people. We


carry out inspe


ction, so must go


dee


p among t


he masses, go


dee


p into t


he realitie


s, always


pay attention to the


people's livel


ihood, to grasp t


he


publ


ic sentiment, a


nd e


arnestly


safeguard t


he be


nefit, addressi


ng the masses are m


ost concerne


d about a


nd refle


cting the stronge


st issues, efforts to


solve t


he pr


oblem


of deci


sions impl


emented a


nd


not implemented. One is to


stick to


principl


es. Rig


ht of i


nspecti


on is


one


of the most important


pow


ers of the


Office, should


not


only dare to use,


but also with


cauti


on. So


-calle


d


dared to


use, i


s to hold a


number of important i


ssue


s, bold


supervisi


on ov


er supervisi


on, tra


ck inspe


ction, problems are


not s


olved


do not pass, the


blame does


not hold


did


not miss,


dissatisfaction of the masses di


d not miss, the real right of superv


sion authority,


with the


benefits. Call wit


h ca


uti


on, is


supervisi


ng de


partments should stre


ngthe


n the


consci


ousne


ss of aut


horize


d strictly a


ccordi


ng to pr


oce


dure,


preventi


ng the supervi


sion and excessive to preve


nt adding burde


n to grass


-roots. To thi


s end, the


supervisi


on De


partment of the


Party Committee of supervi


sion must be under city


and County party Committee Secretary


-General (Office). Second, we should focus on. Is the Gover


nor, those relate


d to the gl


obalEve


nt, Gover


nor the protra


cted diff


icult, strong Gover


nor


duri


ng emergency


urgent.


Not havi


ng special


departments in


charge


of the Ge


neral Gover


nor, under t


he normal proce


dure


can


do g


ood thing


s not


Governor,


not a


uthorized


by County lea


ders,


not the


Gover


nor.


Third i


s to solve


the problem. The pur


pose of supervi


sion, to resolve the pr


oblem.


To a


dher


e to and further impr


ove the


成射线束,经阳极电压加速后射向聚光 镜,起到对电子束加速、加压的作用。



聚光镜:将

< p>
电子束聚集,可用已控制照明强度和孔径角。



样 品室:放置待观察的样品,


并装有倾转台,


用以改变试样的角度 ,还有装配加热、冷却等设备。



物镜:为放大率很高的短距透 镜,作


用是放大电子像。物镜是决定透射电子显微镜分辨能力和成像质量的关键。



中间镜:为可


变倍的弱透镜,


作用是对电子像进行二次放大。


通过调节中间镜的电流,

可选择物体的像或


电子衍射图来进行放大。



透射镜:为高倍的强透镜,用来放大中间像后在荧光屏上成像。



此外还有二级真空泵来对样品室抽真空、照相装置用以记录影像。



应用





透射电子显微镜在材料科学、


生物学上应用较多。


由于电子易散射或被物体吸收,


故穿


透力低,样品的 密度、厚度等都会影响到最后的成像质量,必须制备更薄的超薄切片,


通常



50



100nm



所以用透射电子显微镜观察时的样品需要处理得很薄。


常用的方法有:


超薄


切片法、冷冻超薄切片法、冷冻 蚀刻法、冷冻断裂法等。对于液体样品,通常是挂预处理过


的铜网上进行观察。




特点





TEM


常 用于研究纳米材料的结晶情况,观察纳米粒子的形貌、分散情况及测量和评


估纳米粒子的 粒径。是常用的纳米复合材料微观结构的表征技术之一。






以电子束作光源,电磁场作透镜。 电子束波长与加速电压


(


通常


50~1 20KV)


的平方根


成反比。






由电子 照明系统、


电磁透镜成像系统、


真空系统、

记录系统、


电源系统等


5


部分构成 。





< /p>


分辨力


0.2nm


,放大倍数可达百万倍 。





< /p>


TEM


分析技术是以波长极短的电子束作照明源,用电磁透镜聚焦 成像的一种高分辨


率(


1nm



、高放大倍数的电子光学分析技术;






用电镜(包括

TEM


)进行样品分析时,通常有两个目的:一个是获得高倍放大倍数


的电子图像,另一个是得到电子衍射花样;






TEM


常 用于研究纳米材料的结晶情况,观察纳米粒子的形貌、分散情况及测量和评


估纳米粒子的 粒径。是常用的纳米复合材料微观结构的表征技术之一。



TG





热重




< /p>


热重分析


中的待测物质重量值,相应的有


TGA



DTG


TGA


为热失重分析,即


在温度不断变化的情况下通过仪器 测定其重量的变化。


DTG


表示热重的微分。可以用来


分析物质在温度不断变化的情况下重量的变化情况。


DTG


曲线向下为失重峰


——


这最为常

见,向上为增重峰。



XRF


目录


[


隐藏


]


1.


什么是


XRF?

< br>



2.X


射线荧光的物理原理:




eelings survey,


by looki


ng up publi


c se


ntiments to fi


nd pr


obl


ems. Pr


oblems


will increase


its special


supervisi


on,


set up accounts,


hol


d on to it. We


shoul


d conscie


ntiously impleme


nt the lea


ding


contra


cting matters, se


cure


d, ha


d a


n answer to everything, t


hen


settles rate of 100%. Have an im


pact


on some of the


outsta


ndi


ng issues,


supervisi


on


department


s and information component


s togethe


r, play t


he supervi


sory rol


e of the


news me


dia to


promote pr


obl


em solvi


ng. Inve


stee 3. i


nsist


on a


daily run, around the


practi


ce of truth


catching efficie


ncy, focus spe


cification. To give full play to the


party Office around connecting, coordi


nating i


nternal a


nd exter


nal features,


contact, rally at all level


s, to motivate every a


spe


ct, adhere to t


he trut


h, strengt


heni


ng standardized manag


ement to a


chieve


coherent,


efficient and effective functioning


of the da


ily work


of the Party Committee. Is


processing messages should


strive to streamline, standardize and quality.


Streamlining is to control the number


of


messages, compress message


s, reduci


ng procedures, im


prove messag


e ha


ndli


ng efficiency. S


pecifications, is t


o strictly e


nforce the ba


n issued


by the Communi


st party aut


horitie


s in document


handling reg


ulations a


nd pr


ovincial and munici


pal regulati


ons, conscienti


ously strengthen


nd impr


ove communications manageme


nt to ensure that


party docume


nts or


derly. High


qualit


y, is t


o improve the quality of message


processi


ng, it is nece


ssary to a


ccurately implementi


ng the i


ntention of the


Party Committee, cl


earance, good


communications,


poli


cy pr


ogram closed, e


nsuring that t


here is


no


error. Second meeting


scheduled to


ensure thoroug


h, safe a


nd efficie


nt. Any arrangeme


nts for the meeti


ngs a


nd eve


nts, carefully arranged, item


-by


-item interface impleme


nted,


sure.


o vigor


ously streamline meeti


ngs, a


ctivities,


number


of pressure reducti


on,


scale t


o ensure that le


adership emer


ged from the Ge


neral Conference and entertai


nment servi


ces, focus on big thi


ngs, matters. T


hird, re


cepti


on


service


s


should lay


stress


on


huma


ne,


personal,


cult


ural and human. Recepti


on


and work


directly


with


people, re


cepti


on


services directly affecting t


he Office


of party


Committee The image of the


region. At the


same time stre


ngthe


ning the constr


ucti


on


of library, improve t


he re


cepti


on


conditi


ons, more


human


-ori


ented, persona


l, cultural w


ork int


o the re


ce


ption, a little more


huma


n needs, a little more


human care more


humane atmospher


e, and constantly impr


ove the


service, improv


e the


quality


of servi


ce. M


eanw


hile, t


o further pay spe


cial attention to t


he


daily w


ork of the


oth


er Office Syst


em. Confidential


work re


sponsibility sy


stem for leadi


ng ca


dres to implement


security as


a leade


r, to


improve t


he confidentiality


of classified personnel


, especi


ally leadi


ng ca


dres,


strengthening


party a


nd Governme


nt focus


on vital


sect


ors of security management, to adva


nce priva


cy manageme


nt standar


dization, modernization of se


curity te


chniques a


s a mea


ns of a


dministration accor


ding t


o law a


nd


securi ty


enforceme


nt, ensure the


safety of the party and State secrets. Confide


ntial work to meet the dema


nds


of new technology


develo


pment

-


-


-


-


-


-


-


-



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